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New! 900 MHz Data from 1.6mm HFXY PhoenixNMR Probe

May 29th, 2020 Posted by PhoenixNMR, Products, Technology No Comment yet

Below: aliphatic region of the 2D CC spectrum of 15N, 13C labeled alpha-synuclein protein monomer seeded from a brain tissue sample (250 ms CORD mixing), acquired at 900 MHz 1H field at the National Magnetic Resonance Facility at Madison (NMRFAM, @NMRFAM) , utilizing a PhoenixNMR HFXY probe fitted with a 1.6mm module and PhoenixNMR speed controller (PMAS).

The PhoenixNMR HFXY probe was operated in double resonance mode at MASS = 20 kHz; mixing time = 250 ms; total time to acquire spectrum = 20 hrs using 4 blocks of 1024 rows each; 8 acquisitions per row; pulse delay = 1.5 s; CORDxy4 recoupling plus SPINAL decoupling.

Expansion of 900 MHZ CC Aliphatic Correlation Data NMRFAM
Expansion of a Near-Diagonal Region of the 2D CC spectrum
Second Expansion of 900 MHZ CC Aliphatic Correlation Data NMRFAM
A second Expansion of a near-diagonal region of the 2D CC Spectrum. Note the excellent lineshape provided by the PhoenixNMR probe demonstrated by both of these expansions.

Data courtesy Prof. Chad M. Rienstra, Dr. Marco Tonelli and Dr. Dwaipayan Mukhopadhyay. Data were acquired at the National Magnetic Resonance Facility at Madison ( NMRFAM, @NMRFAM). This 900 MHz SSNMR instrument and probe are available for use at NMRFAM by any scientist worldwide.

For more information about the PhoenixNMR HFXY Probe or PMAS Controller:

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February 27th, 2014 Posted by PhoenixNMR No Comment yet

Phoenix NMR is driven by experience and knowledge to design, manufacture, and service the highest-quality Solid State Nuclear Magnetic Resonance probes in the marketplace.  (more…)